NMR for polymorphism

Mollica Lab

    								
     
    2022
  1. 
    Supercritical CO2 impregnation process applied to polymer samples preparation for dynamic nuclear polarization solid-state NMR
    

    

Magnetic Resonance in Chemistry, 2022, 60, p.1171-1177
    


    D. Le, A. Frison, Y. Masmoudi, A. Bouledjouidja, P. Thureau, G. Mollica, E. Badens, F. Ziarelli, S. Viel
  2. 
    Monitoring the influence of additives on the crystallization processes of glycine with dynamic nuclear polarization solid-state NMR
    

    

Solid-state Nuclear Magnetic Resonance, 2022, 122, p.101836
    


    M. Juramy, P. Cerreia-Vioglio, F. Ziarelli, S. Viel, P. Thureau, G. Mollica*
  3. 
    Recent progress in nuclear magnetic resonance strategies for time-resolved atomic-level investigation of crystallization from solution
    

    

Current Opinion in Colloid Interface & Science, 2022, , p.accepted
    


    M. Juramy, G. Mollica*
    4. 								
     
    2021
  4. 
    Monitoring crystallization processes in confined porous materials by dynamic nuclear polarization solid-state nuclear magnetic resonance
    

    

Journal of the American Chemical Society, 2021, 143, p.6095-6103
    


    M. Juramy, R. Chèvre, P. Cerreia-Vioglio, F. Ziarelli, E. Besson, S. Gastaldi, S. Viel, P. Thureau, K. D. M. Harris, G. Mollica*
    5. 								
     
    2020
  5. 
    Solvent suppression in solid-state DNP NMR using Electronic Mixing-Mediated Annihilation (EMMA)
    

    

Magnetic Resonance in Chemistry, 2020, 58, p.1076-1081
    


    F. Ziarelli, P. Thureau, S. Viel, G. Mollica*
    6. 								
     
    2019
  6. 
    Chapter 22: Structural Investigations of Polymer Materials by Dynamic Nuclear Polarisation Solid-state NMR
    

    

Book Chapter- NMR Methods for Characterization of Synthetic and Natural Polymers, 2019, , p.533-554
    


    G. Mollica, F. Ziarelli, P. Thureau, S. Viel
  7. 
    A Karplus equation for the conformational analysis of organic molecular crystals
    

    

Angewandte Chemie International Edition, 2019, 58, p.16047-16051
    


    P. Thureau, I. Carvin, F. Ziarelli, S. Viel, G. Mollica*
  8. 
    Reducing the computational cost of NMR crystallography of organic powders at natural isotopic abundance with the help of 13C-13C dipolar couplings
    

    

Magnetic Resonance in Chemistry, 2019, 57, p.256-264
    


    P. Thureau, S. Sturniolo, M. Zilka, F. Ziarelli, S. Viel, J. R. Yates, G. Mollica*
  9. 
    A strategy for probing the evolution of crystallization processes by low-temperature solid-state NMR and dynamic nuclear polarization
    

    

The Journal of Physical Chemistry Letters, 2019, 10, p.1505-1510
    


    P. Cerreia-Vioglio, P. Thureau, M. Juramy, F. Ziarelli, S. Viel, P. A. Williams, C. E. Hughes, K. D. M. Harris, G. Mollica*
    10. 								
     
    2018
  10. 
    Insights into the crystallization and structural evolution of glycine dihydrate by in situ solid-state NMR spectroscopy
    

    

Angewandte Chemie International Edition, 2018, 57, p.6619-6623
    


    P. Cerreia Vioglio, G. Mollica, M. Juramy, C. E. Hughes, P. A. Williams, F. Ziarelli, S. Viel, P. Thureau, K. D. M. Harris
    11. 								
     
    2016
  11. 
    Determining carbon-carbon connectivities in natural abundance organic powders using dipolar couplings
    

    

Chemical Communications, 2016, 52, p.8565-8568
    


    M. Dekhil, G. Mollica, T. Texier-Bonniot, F. Ziarelli, P. Thureau, S. Viel
    12. 								
     
    2015
  12. 
    Up to 100% Improvement in Dynamic Nuclear Polarization Solid-State {NMR} Sensitivity Enhancement of Polymers by Removing Oxygen
    

    

Macromolecular Rapid Communications, 2015, 36, p.1416-1421
    


    D. Le, F. Ziarelli, T.N.T Phan, G. Mollica, P. Thureau, F. Aussenac, O. Ouari, D. Gigmes, P. Tordo, S. Viel
  13. 
    Quantitative Structural Constraints for Organic Powders at Natural Isotopic Abundance Using Dynamic Nuclear Polarization Solid-State NMR Spectroscopy
    

    

Angewandte Chemie-International Edition, 2015, 54, p.6028-6031
    


    G. Mollica, M. Dekhil, F. Ziarelli, P. Thureau, S. Viel
  14. 
    Probing crystal packing of uniformly 13C-enriched powder samples using homonuclear dipolar coupling measurements
    

    

Solid State Nuclear Magnetic Resonance, 2015, 65, p.114-21
    


    G. Mollica, M. Dekhil, F. Ziarelli, P. Thureau, S. Viel
    15. 								
     
    2014
  15. 
    Optimizing Sample Preparation Methods for Dynamic Nuclear Polarization Solid-state NMR of Synthetic Polymers
    

    

Macromolecules, 2014, 47, p.3909-3916
    


    D. Le, G. Casano, T. N. Phan, F. Ziarelli, O. Ouari, F. Aussenac, P. Thureau, G. Mollica, D. Gigmes, P. Tordo, S. Viel
  16. 
    Observing Apparent Nonuniform Sensitivity Enhancements in Dynamic Nuclear Polarization Solid-State NMR Spectra of Polymers
    

    

ACS Macro Letters, 2014, 3, p.922-925
    


    G. Mollica, D. Le, F. Ziarelli, G. Casano, O. Ouari, T. N. T. Phan, F. Aussenac, P. Thureau, D. Gigmes, P. Tordo, S. Viel
  17. 
    Chapter Five: Solid-State 1H NMR Studies of Homonuclear Dipolar Couplings
    

    

Book Chapter - Annual Reports on NMR Spectroscopy, 2014, , p.217-249
    


    P. Thureau, G. Mollica, F. Ziarelli, S. Viel
    18. 								
     
    2013
  18. 
    Selective measurements of long-range homonuclear J-couplings in solid-state NMR
    

    

Journal of Magnetic Resonance, 2013, 231, p.90-4
    


    P. Thureau, G. Mollica, F. Ziarelli, S. Viel
    19. 								
     
    2012
  19. 
    Towards the rationalization of the MALDI process: a combined mass spectrometry/solid-state NMR approach
    

    

Analytical Methods, 2012, 4, p.3118
    


    Y. Major, H. Pizzala, F. Ziarelli, T. N. T. Phan, G. Mollica*, L. Charles
  20. 
    Towards measurement of homonuclear dipolar couplings in 1H solid-state NMR: recoupling with a rotor-synchronized decoupling scheme
    

    

Physical Chemistry Chemical Physics, 2012, 14, p.4359-64
    


    G. Mollica, P. K. Madhu, F. Ziarelli, A. Thevand, P. Thureau, S. Viel
  21. 
    Suppressing background signals in solid state NMR via the Electronic Mixing-Mediated Annihilation (EMMA) method
    

    

Journal of Magnetic Resonance, 2012, 218, p.1-4
    


    G. Mollica, F. Ziarelli, A. Tintaru, P. Thureau, S. Viel
  22. 
    Probing the motional behavior of eumelanin and pheomelanin with solid-state NMR spectroscopy: new insights into the pigment properties
    

    

Chemistry- A European Journal, 2012, 18, p.10689-700
    


    P. Thureau, F. Ziarelli, A. Thevand, R. W. Martin, P. Farmer, S. Viel, G. Mollica*
  23. 
    Characterization of insoluble calcium alginates by solid-state NMR
    

    

Carbohydrate Polymers, 2012, 87, p.383-391
    


    G. Mollica*, F. Ziarelli, S. Lack, F. Brunel, S. Viel
    24. 								
     
    2011
  24. 
    Solid-state nuclear magnetic resonance characterization of PE-PEG/silica hybrid materials prepared by microwave-assisted sol-gel process
    

    

Journal of Materials Research, 2011, 22, p.3516-3525
    


    M. Geppi,  G. Mollica, S. Borsacchi, M. Marini, M. Toselli, F. Pilati
  25. 
    Dynamics of ethylene-propylene random copolymers by 1H and 13C solid-state NMR
    

    

Journal of Physical Chemistry B, 2011, 115, p.
    


    G. Mollica, C. Forte, M. Malvaldi, M. Geppi
    26. 								
     
    2010
  26. 
    Proton spin-lattice relaxation in silkworm cocoons: physisorbed water and serine side-chain motions
    

    

Journal of Physical Chemistry B, 2010, 114, p.
    


    M. Geppi, G. Mollica, S. Borsacchi, S. Cappellozza
    27. 								
     
    2009
  27. 
    Applications of Solid-state NMR to the Study of Organic/Inorganic Multicomponent Materials
    

    

Applied Spectroscopy Reviews, 2009, 44, p.1--89
    


    M. Geppi, S. Borsacchi, G. Mollica, C. A. Veracini
    28. 								
     
    2008
  28. 
    Estimation of internuclear couplings in the solid-state NMR of multiple-spin systems. Selective spin echoes and off-magic-angle sample spinning
    

    

Chemical Physics Letters, 2008, 456, p.116-121
    


    G. Pileio, S. Mamone, G. Mollica, I. Montesinos, A. Gansmuller, M. Carravetta, S.P. Brown, M. H. Levitt
  29. 
    Solid-state NMR of Organic/Inorganic Multicomponent Materials
    

    

Encyclopedia of Nuclear Magnetic Resonance, 2008, , p.
    


    M. Geppi, S. Borsacchi, G. Mollica
  30. 
    Solid-State NMR studies of Pharmaceutical Systems
    

    

Applied Spectroscopy Reviews, 2008, 43, p.202--302
    


    M. Geppi, G. Mollica, S. Borsacchi, C. A. Veracini
  31. 
    Facile Synthesis of Core-Shell Organic-Inorganic Hybrid Nanoparticles with Amphiphilic Polymer Shell by One-Step Sol-Gel Reactions
    

    

Journal of Polymer Science Polymer Chemistry, 2008, 46, p.1699--1709
    


    M. Marini, M. Toselli, S. Borsacchi, G. Mollica, M. Geppi, F. Pilati
    32. 								
     
    2007
  32. 
    Cotton fibers encapsulated with homo- and block copolymers: Synthesis by the atom transfer radical polymerization grafting-from technique and solid-state NMR dynamic investigations
    

    

Biomacromolecules, 2007, 8, p.498-508
    


    V. Castelvetro, M. Geppi, S. Giaiacopi, G. Mollica
  33. 
    A Novel Polyelectrolyte Complex (PEC) Hydrogel for Controlled Drug Delivery to the Distal Intestine
    

    

The Open Drug Delivery Journal, 2007, 1, p.68-75
    


    C. Zaino, Y. Zambito, G. Mollica, M. Geppi, M. F. Serafini, V. Carelli, G. Di Colo
  34. 
    Solid-state nuclear magnetic resonance characterization of PE-PEG/Silica hybrid materials prepared by microwave-assisted sol-gel process
    

    

Journal of Materials Research, 2007, 22, p.3516-3525
    


    M. Geppi, G. Mollica, S. Borsacchi, M. Marini, M. Toselli, F. Pilati
    35. 								
     
    2006
  35. 
    Molecular properties of flurbiprofen and its solid dispersions with Eudragit RL100 studied by high- and low-resolution solid-state nuclear magnetic resonance
    

    

Pharmaceutical Research, 2006, 23, p.2129-40
    


    G. Mollica, M. Geppi, R. Pignatello, C. A. Veracini
  36. 
    Truncated dipolar recoupling in solid-state nuclear magnetic resonance
    

    

Chemical Physics Letters, 2006, 432, p.572-578
    


    I. Marin-Montesinos, G. Mollica, M. Carravetta, A. Gansmüller, G. Pileio, M. Bechmann, A. Sebald, M. H. Levitt
  37. 
    A new hydrogel for the extended and complete prednisolone release in the GI tract
    

    

International Journal of Pharmaceutics, 2006, 310, p.154-161
    


    G. Di Colo, A. Baggiani, Y. Zambito, G. Mollica, M. Geppi, M. F. Serafini
    38. 								
     
    2005
  38. 
    Molecular properties of ibuprofen and its solid dispersions with Eudragit RL100 studied by solid-state nuclear magnetic resonance
    

    

Pharmaceutical Research, 2005, 22, p.1544-1555
    


    M. Geppi, S. Guccione, G. Mollica, R. Pignatello, C.A. Veracini
    39. 								
     
    2004
  39. 
    Structure and dynamics of flour by solid state NMR: Effects of hydration and wheat aging
    

    

Biomacromolecules, 2004, 5, p.1536-1544
    


    L. Calucci, L. Galleschi, M. Geppi, G. Mollica
		

				

						

					

		

								

					

		

				

						

							

					

			

							

								

					

		

								

					

		

									

			

					

				

					

								

						

							

					

			

							

						

				

					

		
giulia.mollica@univ-amu.fr