NMR for polymorphism

Mollica Lab

    								
     
    2023
  1. 
    Exploiting solid-state dynamic nuclear polarization NMR spectroscopy to establish the spatial distribution of polymorphic phases in a solid material
    

    

Chemical Science, 2023, 14, p.10121 - 10128
    


    S.F. Cousin, C.E. Hughes, F. Ziarelli, S. Viel, G. Mollica*, K.D.M. Harris, A.C. Pinon, P. Thureau
  2. 
    Polarization Amplification in Dynamic Nuclear Polarization Magic- Angle Spinning Solid-State Nuclear Magnetic Resonance by Solubilizing Traditional Ionic Salts
    

    

J. Phys. Chem. Lett., 2023, , p.accepted
    


    F. Ferrer, M. Juramy, R. Jabbour, S. Cousin, F. Ziarelli, G. Mollica, P. Thureau, S. Viel.
  3. 
    Recent progress in nuclear magnetic resonance strategies for time-resolved atomic-level investigation of crystallization from solution
    

    

Current Opinion in Colloid Interface & Science, 2023, 63, p.101663
    


    M. Juramy, G. Mollica*
    4. 								
     
    2022
  4. 
    Supercritical CO2 impregnation process applied to polymer samples preparation for dynamic nuclear polarization solid-state NMR
    

    

Magnetic Resonance in Chemistry, 2022, 60, p.1171-1177
    


    D. Le, A. Frison, Y. Masmoudi, A. Bouledjouidja, P. Thureau, G. Mollica, E. Badens, F. Ziarelli, S. Viel
  5. 
    Monitoring the influence of additives on the crystallization processes of glycine with dynamic nuclear polarization solid-state NMR
    

    

Solid-state Nuclear Magnetic Resonance, 2022, 122, p.101836
    


    M. Juramy, P. Cerreia-Vioglio, F. Ziarelli, S. Viel, P. Thureau, G. Mollica*
    6. 								
     
    2021
  6. 
    Monitoring crystallization processes in confined porous materials by dynamic nuclear polarization solid-state nuclear magnetic resonance
    

    

Journal of the American Chemical Society, 2021, 143, p.6095-6103
    


    M. Juramy, R. Chèvre, P. Cerreia-Vioglio, F. Ziarelli, E. Besson, S. Gastaldi, S. Viel, P. Thureau, K. D. M. Harris, G. Mollica*
    7. 								
     
    2020
  7. 
    Solvent suppression in solid-state DNP NMR using Electronic Mixing-Mediated Annihilation (EMMA)
    

    

Magnetic Resonance in Chemistry, 2020, 58, p.1076-1081
    


    F. Ziarelli, P. Thureau, S. Viel, G. Mollica*
    8. 								
     
    2019
  8. 
    Chapter 22: Structural Investigations of Polymer Materials by Dynamic Nuclear Polarisation Solid-state NMR
    

    

Book Chapter- NMR Methods for Characterization of Synthetic and Natural Polymers, 2019, , p.533-554
    


    G. Mollica, F. Ziarelli, P. Thureau, S. Viel
  9. 
    A Karplus equation for the conformational analysis of organic molecular crystals
    

    

Angewandte Chemie International Edition, 2019, 58, p.16047-16051
    


    P. Thureau, I. Carvin, F. Ziarelli, S. Viel, G. Mollica*
  10. 
    Reducing the computational cost of NMR crystallography of organic powders at natural isotopic abundance with the help of 13C-13C dipolar couplings
    

    

Magnetic Resonance in Chemistry, 2019, 57, p.256-264
    


    P. Thureau, S. Sturniolo, M. Zilka, F. Ziarelli, S. Viel, J. R. Yates, G. Mollica*
  11. 
    A strategy for probing the evolution of crystallization processes by low-temperature solid-state NMR and dynamic nuclear polarization
    

    

The Journal of Physical Chemistry Letters, 2019, 10, p.1505-1510
    


    P. Cerreia-Vioglio, P. Thureau, M. Juramy, F. Ziarelli, S. Viel, P. A. Williams, C. E. Hughes, K. D. M. Harris, G. Mollica*
    12. 								
     
    2018
  12. 
    Insights into the crystallization and structural evolution of glycine dihydrate by in situ solid-state NMR spectroscopy
    

    

Angewandte Chemie International Edition, 2018, 57, p.6619-6623
    


    P. Cerreia Vioglio, G. Mollica, M. Juramy, C. E. Hughes, P. A. Williams, F. Ziarelli, S. Viel, P. Thureau, K. D. M. Harris
    13. 								
     
    2016
  13. 
    Determining carbon-carbon connectivities in natural abundance organic powders using dipolar couplings
    

    

Chemical Communications, 2016, 52, p.8565-8568
    


    M. Dekhil, G. Mollica, T. Texier-Bonniot, F. Ziarelli, P. Thureau, S. Viel
    14. 								
     
    2015
  14. 
    Up to 100% Improvement in Dynamic Nuclear Polarization Solid-State {NMR} Sensitivity Enhancement of Polymers by Removing Oxygen
    

    

Macromolecular Rapid Communications, 2015, 36, p.1416-1421
    


    D. Le, F. Ziarelli, T.N.T Phan, G. Mollica, P. Thureau, F. Aussenac, O. Ouari, D. Gigmes, P. Tordo, S. Viel
  15. 
    Quantitative Structural Constraints for Organic Powders at Natural Isotopic Abundance Using Dynamic Nuclear Polarization Solid-State NMR Spectroscopy
    

    

Angewandte Chemie-International Edition, 2015, 54, p.6028-6031
    


    G. Mollica, M. Dekhil, F. Ziarelli, P. Thureau, S. Viel
  16. 
    Probing crystal packing of uniformly 13C-enriched powder samples using homonuclear dipolar coupling measurements
    

    

Solid State Nuclear Magnetic Resonance, 2015, 65, p.114-21
    


    G. Mollica, M. Dekhil, F. Ziarelli, P. Thureau, S. Viel
    17. 								
     
    2014
  17. 
    Optimizing Sample Preparation Methods for Dynamic Nuclear Polarization Solid-state NMR of Synthetic Polymers
    

    

Macromolecules, 2014, 47, p.3909-3916
    


    D. Le, G. Casano, T. N. Phan, F. Ziarelli, O. Ouari, F. Aussenac, P. Thureau, G. Mollica, D. Gigmes, P. Tordo, S. Viel
  18. 
    Observing Apparent Nonuniform Sensitivity Enhancements in Dynamic Nuclear Polarization Solid-State NMR Spectra of Polymers
    

    

ACS Macro Letters, 2014, 3, p.922-925
    


    G. Mollica, D. Le, F. Ziarelli, G. Casano, O. Ouari, T. N. T. Phan, F. Aussenac, P. Thureau, D. Gigmes, P. Tordo, S. Viel
  19. 
    Chapter Five: Solid-State 1H NMR Studies of Homonuclear Dipolar Couplings
    

    

Book Chapter - Annual Reports on NMR Spectroscopy, 2014, , p.217-249
    


    P. Thureau, G. Mollica, F. Ziarelli, S. Viel
    20. 								
     
    2013
  20. 
    Selective measurements of long-range homonuclear J-couplings in solid-state NMR
    

    

Journal of Magnetic Resonance, 2013, 231, p.90-4
    


    P. Thureau, G. Mollica, F. Ziarelli, S. Viel
    21. 								
     
    2012
  21. 
    Towards the rationalization of the MALDI process: a combined mass spectrometry/solid-state NMR approach
    

    

Analytical Methods, 2012, 4, p.3118
    


    Y. Major, H. Pizzala, F. Ziarelli, T. N. T. Phan, G. Mollica*, L. Charles
  22. 
    Towards measurement of homonuclear dipolar couplings in 1H solid-state NMR: recoupling with a rotor-synchronized decoupling scheme
    

    

Physical Chemistry Chemical Physics, 2012, 14, p.4359-64
    


    G. Mollica, P. K. Madhu, F. Ziarelli, A. Thevand, P. Thureau, S. Viel
  23. 
    Suppressing background signals in solid state NMR via the Electronic Mixing-Mediated Annihilation (EMMA) method
    

    

Journal of Magnetic Resonance, 2012, 218, p.1-4
    


    G. Mollica, F. Ziarelli, A. Tintaru, P. Thureau, S. Viel
  24. 
    Probing the motional behavior of eumelanin and pheomelanin with solid-state NMR spectroscopy: new insights into the pigment properties
    

    

Chemistry- A European Journal, 2012, 18, p.10689-700
    


    P. Thureau, F. Ziarelli, A. Thevand, R. W. Martin, P. Farmer, S. Viel, G. Mollica*
  25. 
    Characterization of insoluble calcium alginates by solid-state NMR
    

    

Carbohydrate Polymers, 2012, 87, p.383-391
    


    G. Mollica*, F. Ziarelli, S. Lack, F. Brunel, S. Viel
    26. 								
     
    2011
  26. 
    Solid-state nuclear magnetic resonance characterization of PE-PEG/silica hybrid materials prepared by microwave-assisted sol-gel process
    

    

Journal of Materials Research, 2011, 22, p.3516-3525
    


    M. Geppi,  G. Mollica, S. Borsacchi, M. Marini, M. Toselli, F. Pilati
  27. 
    Dynamics of ethylene-propylene random copolymers by 1H and 13C solid-state NMR
    

    

Journal of Physical Chemistry B, 2011, 115, p.
    


    G. Mollica, C. Forte, M. Malvaldi, M. Geppi
    28. 								
     
    2010
  28. 
    Proton spin-lattice relaxation in silkworm cocoons: physisorbed water and serine side-chain motions
    

    

Journal of Physical Chemistry B, 2010, 114, p.
    


    M. Geppi, G. Mollica, S. Borsacchi, S. Cappellozza
    29. 								
     
    2009
  29. 
    Applications of Solid-state NMR to the Study of Organic/Inorganic Multicomponent Materials
    

    

Applied Spectroscopy Reviews, 2009, 44, p.1--89
    


    M. Geppi, S. Borsacchi, G. Mollica, C. A. Veracini
    30. 								
     
    2008
  30. 
    Estimation of internuclear couplings in the solid-state NMR of multiple-spin systems. Selective spin echoes and off-magic-angle sample spinning
    

    

Chemical Physics Letters, 2008, 456, p.116-121
    


    G. Pileio, S. Mamone, G. Mollica, I. Montesinos, A. Gansmuller, M. Carravetta, S.P. Brown, M. H. Levitt
  31. 
    Solid-state NMR of Organic/Inorganic Multicomponent Materials
    

    

Encyclopedia of Nuclear Magnetic Resonance, 2008, , p.
    


    M. Geppi, S. Borsacchi, G. Mollica
  32. 
    Solid-State NMR studies of Pharmaceutical Systems
    

    

Applied Spectroscopy Reviews, 2008, 43, p.202--302
    


    M. Geppi, G. Mollica, S. Borsacchi, C. A. Veracini
  33. 
    Facile Synthesis of Core-Shell Organic-Inorganic Hybrid Nanoparticles with Amphiphilic Polymer Shell by One-Step Sol-Gel Reactions
    

    

Journal of Polymer Science Polymer Chemistry, 2008, 46, p.1699--1709
    


    M. Marini, M. Toselli, S. Borsacchi, G. Mollica, M. Geppi, F. Pilati
    34. 								
     
    2007
  34. 
    Cotton fibers encapsulated with homo- and block copolymers: Synthesis by the atom transfer radical polymerization grafting-from technique and solid-state NMR dynamic investigations
    

    

Biomacromolecules, 2007, 8, p.498-508
    


    V. Castelvetro, M. Geppi, S. Giaiacopi, G. Mollica
  35. 
    A Novel Polyelectrolyte Complex (PEC) Hydrogel for Controlled Drug Delivery to the Distal Intestine
    

    

The Open Drug Delivery Journal, 2007, 1, p.68-75
    


    C. Zaino, Y. Zambito, G. Mollica, M. Geppi, M. F. Serafini, V. Carelli, G. Di Colo
  36. 
    Solid-state nuclear magnetic resonance characterization of PE-PEG/Silica hybrid materials prepared by microwave-assisted sol-gel process
    

    

Journal of Materials Research, 2007, 22, p.3516-3525
    


    M. Geppi, G. Mollica, S. Borsacchi, M. Marini, M. Toselli, F. Pilati
    37. 								
     
    2006
  37. 
    Molecular properties of flurbiprofen and its solid dispersions with Eudragit RL100 studied by high- and low-resolution solid-state nuclear magnetic resonance
    

    

Pharmaceutical Research, 2006, 23, p.2129-40
    


    G. Mollica, M. Geppi, R. Pignatello, C. A. Veracini
  38. 
    Truncated dipolar recoupling in solid-state nuclear magnetic resonance
    

    

Chemical Physics Letters, 2006, 432, p.572-578
    


    I. Marin-Montesinos, G. Mollica, M. Carravetta, A. Gansmüller, G. Pileio, M. Bechmann, A. Sebald, M. H. Levitt
  39. 
    A new hydrogel for the extended and complete prednisolone release in the GI tract
    

    

International Journal of Pharmaceutics, 2006, 310, p.154-161
    


    G. Di Colo, A. Baggiani, Y. Zambito, G. Mollica, M. Geppi, M. F. Serafini
    40. 								
     
    2005
  40. 
    Molecular properties of ibuprofen and its solid dispersions with Eudragit RL100 studied by solid-state nuclear magnetic resonance
    

    

Pharmaceutical Research, 2005, 22, p.1544-1555
    


    M. Geppi, S. Guccione, G. Mollica, R. Pignatello, C.A. Veracini
    41. 								
     
    2004
  41. 
    Structure and dynamics of flour by solid state NMR: Effects of hydration and wheat aging
    

    

Biomacromolecules, 2004, 5, p.1536-1544
    


    L. Calucci, L. Galleschi, M. Geppi, G. Mollica
		

				

					

		

							

		

				

						

					

			

									

		

							

		

							

				

								

						

					

			

								

				

					

		
giulia.mollica@univ-amu.fr