2023

  1. Exploiting solid-state dynamic nuclear polarization NMR spectroscopy to establish the spatial distribution of polymorphic phases in a solid material
    Chemical Science, 2023, 14, p.10121 - 10128

    S.F. Cousin, C.E. Hughes, F. Ziarelli, S. Viel, G. Mollica*, K.D.M. Harris, A.C. Pinon, P. Thureau

  2. Polarization Amplification in Dynamic Nuclear Polarization Magic- Angle Spinning Solid-State Nuclear Magnetic Resonance by Solubilizing Traditional Ionic Salts
    J. Phys. Chem. Lett., 2023, , p.accepted

    F. Ferrer, M. Juramy, R. Jabbour, S. Cousin, F. Ziarelli, G. Mollica, P. Thureau, S. Viel.

  3. Recent progress in nuclear magnetic resonance strategies for time-resolved atomic-level investigation of crystallization from solution
    Current Opinion in Colloid Interface & Science, 2023, 63, p.101663

    M. Juramy, G. Mollica*

  4. 2022

  5. Supercritical CO2 impregnation process applied to polymer samples preparation for dynamic nuclear polarization solid-state NMR
    Magnetic Resonance in Chemistry, 2022, 60, p.1171-1177

    D. Le, A. Frison, Y. Masmoudi, A. Bouledjouidja, P. Thureau, G. Mollica, E. Badens, F. Ziarelli, S. Viel

  6. Monitoring the influence of additives on the crystallization processes of glycine with dynamic nuclear polarization solid-state NMR
    Solid-state Nuclear Magnetic Resonance, 2022, 122, p.101836

    M. Juramy, P. Cerreia-Vioglio, F. Ziarelli, S. Viel, P. Thureau, G. Mollica*

  7. 2021

  8. Monitoring crystallization processes in confined porous materials by dynamic nuclear polarization solid-state nuclear magnetic resonance
    Journal of the American Chemical Society, 2021, 143, p.6095-6103

    M. Juramy, R. Chèvre, P. Cerreia-Vioglio, F. Ziarelli, E. Besson, S. Gastaldi, S. Viel, P. Thureau, K. D. M. Harris, G. Mollica*

  9. 2020

  10. Solvent suppression in solid-state DNP NMR using Electronic Mixing-Mediated Annihilation (EMMA)
    Magnetic Resonance in Chemistry, 2020, 58, p.1076-1081

    F. Ziarelli, P. Thureau, S. Viel, G. Mollica*

  11. 2019

  12. Chapter 22: Structural Investigations of Polymer Materials by Dynamic Nuclear Polarisation Solid-state NMR
    Book Chapter- NMR Methods for Characterization of Synthetic and Natural Polymers, 2019, , p.533-554

    G. Mollica, F. Ziarelli, P. Thureau, S. Viel

  13. A Karplus equation for the conformational analysis of organic molecular crystals
    Angewandte Chemie International Edition, 2019, 58, p.16047-16051

    P. Thureau, I. Carvin, F. Ziarelli, S. Viel, G. Mollica*

  14. Reducing the computational cost of NMR crystallography of organic powders at natural isotopic abundance with the help of 13C-13C dipolar couplings
    Magnetic Resonance in Chemistry, 2019, 57, p.256-264

    P. Thureau, S. Sturniolo, M. Zilka, F. Ziarelli, S. Viel, J. R. Yates, G. Mollica*

  15. A strategy for probing the evolution of crystallization processes by low-temperature solid-state NMR and dynamic nuclear polarization
    The Journal of Physical Chemistry Letters, 2019, 10, p.1505-1510

    P. Cerreia-Vioglio, P. Thureau, M. Juramy, F. Ziarelli, S. Viel, P. A. Williams, C. E. Hughes, K. D. M. Harris, G. Mollica*

  16. 2018

  17. Insights into the crystallization and structural evolution of glycine dihydrate by in situ solid-state NMR spectroscopy
    Angewandte Chemie International Edition, 2018, 57, p.6619-6623

    P. Cerreia Vioglio, G. Mollica, M. Juramy, C. E. Hughes, P. A. Williams, F. Ziarelli, S. Viel, P. Thureau, K. D. M. Harris

  18. 2016

  19. Determining carbon-carbon connectivities in natural abundance organic powders using dipolar couplings
    Chemical Communications, 2016, 52, p.8565-8568

    M. Dekhil, G. Mollica, T. Texier-Bonniot, F. Ziarelli, P. Thureau, S. Viel

  20. 2015

  21. Up to 100% Improvement in Dynamic Nuclear Polarization Solid-State {NMR} Sensitivity Enhancement of Polymers by Removing Oxygen
    Macromolecular Rapid Communications, 2015, 36, p.1416-1421

    D. Le, F. Ziarelli, T.N.T Phan, G. Mollica, P. Thureau, F. Aussenac, O. Ouari, D. Gigmes, P. Tordo, S. Viel

  22. Quantitative Structural Constraints for Organic Powders at Natural Isotopic Abundance Using Dynamic Nuclear Polarization Solid-State NMR Spectroscopy
    Angewandte Chemie-International Edition, 2015, 54, p.6028-6031

    G. Mollica, M. Dekhil, F. Ziarelli, P. Thureau, S. Viel

  23. Probing crystal packing of uniformly 13C-enriched powder samples using homonuclear dipolar coupling measurements
    Solid State Nuclear Magnetic Resonance, 2015, 65, p.114-21

    G. Mollica, M. Dekhil, F. Ziarelli, P. Thureau, S. Viel

  24. 2014

  25. Optimizing Sample Preparation Methods for Dynamic Nuclear Polarization Solid-state NMR of Synthetic Polymers
    Macromolecules, 2014, 47, p.3909-3916

    D. Le, G. Casano, T. N. Phan, F. Ziarelli, O. Ouari, F. Aussenac, P. Thureau, G. Mollica, D. Gigmes, P. Tordo, S. Viel

  26. Observing Apparent Nonuniform Sensitivity Enhancements in Dynamic Nuclear Polarization Solid-State NMR Spectra of Polymers
    ACS Macro Letters, 2014, 3, p.922-925

    G. Mollica, D. Le, F. Ziarelli, G. Casano, O. Ouari, T. N. T. Phan, F. Aussenac, P. Thureau, D. Gigmes, P. Tordo, S. Viel

  27. Chapter Five: Solid-State 1H NMR Studies of Homonuclear Dipolar Couplings
    Book Chapter - Annual Reports on NMR Spectroscopy, 2014, , p.217-249

    P. Thureau, G. Mollica, F. Ziarelli, S. Viel

  28. 2013

  29. Selective measurements of long-range homonuclear J-couplings in solid-state NMR
    Journal of Magnetic Resonance, 2013, 231, p.90-4

    P. Thureau, G. Mollica, F. Ziarelli, S. Viel

  30. 2012

  31. Towards the rationalization of the MALDI process: a combined mass spectrometry/solid-state NMR approach
    Analytical Methods, 2012, 4, p.3118

    Y. Major, H. Pizzala, F. Ziarelli, T. N. T. Phan, G. Mollica*, L. Charles

  32. Towards measurement of homonuclear dipolar couplings in 1H solid-state NMR: recoupling with a rotor-synchronized decoupling scheme
    Physical Chemistry Chemical Physics, 2012, 14, p.4359-64

    G. Mollica, P. K. Madhu, F. Ziarelli, A. Thevand, P. Thureau, S. Viel

  33. Suppressing background signals in solid state NMR via the Electronic Mixing-Mediated Annihilation (EMMA) method
    Journal of Magnetic Resonance, 2012, 218, p.1-4

    G. Mollica, F. Ziarelli, A. Tintaru, P. Thureau, S. Viel

  34. Probing the motional behavior of eumelanin and pheomelanin with solid-state NMR spectroscopy: new insights into the pigment properties
    Chemistry- A European Journal, 2012, 18, p.10689-700

    P. Thureau, F. Ziarelli, A. Thevand, R. W. Martin, P. Farmer, S. Viel, G. Mollica*

  35. Characterization of insoluble calcium alginates by solid-state NMR
    Carbohydrate Polymers, 2012, 87, p.383-391

    G. Mollica*, F. Ziarelli, S. Lack, F. Brunel, S. Viel

  36. 2011

  37. Solid-state nuclear magnetic resonance characterization of PE-PEG/silica hybrid materials prepared by microwave-assisted sol-gel process
    Journal of Materials Research, 2011, 22, p.3516-3525

    M. Geppi, G. Mollica, S. Borsacchi, M. Marini, M. Toselli, F. Pilati

  38. Dynamics of ethylene-propylene random copolymers by 1H and 13C solid-state NMR
    Journal of Physical Chemistry B, 2011, 115, p.

    G. Mollica, C. Forte, M. Malvaldi, M. Geppi

  39. 2010

  40. Proton spin-lattice relaxation in silkworm cocoons: physisorbed water and serine side-chain motions
    Journal of Physical Chemistry B, 2010, 114, p.

    M. Geppi, G. Mollica, S. Borsacchi, S. Cappellozza

  41. 2009

  42. Applications of Solid-state NMR to the Study of Organic/Inorganic Multicomponent Materials
    Applied Spectroscopy Reviews, 2009, 44, p.1--89

    M. Geppi, S. Borsacchi, G. Mollica, C. A. Veracini

  43. 2008

  44. Estimation of internuclear couplings in the solid-state NMR of multiple-spin systems. Selective spin echoes and off-magic-angle sample spinning
    Chemical Physics Letters, 2008, 456, p.116-121

    G. Pileio, S. Mamone, G. Mollica, I. Montesinos, A. Gansmuller, M. Carravetta, S.P. Brown, M. H. Levitt

  45. Solid-state NMR of Organic/Inorganic Multicomponent Materials
    Encyclopedia of Nuclear Magnetic Resonance, 2008, , p.

    M. Geppi, S. Borsacchi, G. Mollica

  46. Solid-State NMR studies of Pharmaceutical Systems
    Applied Spectroscopy Reviews, 2008, 43, p.202--302

    M. Geppi, G. Mollica, S. Borsacchi, C. A. Veracini

  47. Facile Synthesis of Core-Shell Organic-Inorganic Hybrid Nanoparticles with Amphiphilic Polymer Shell by One-Step Sol-Gel Reactions
    Journal of Polymer Science Polymer Chemistry, 2008, 46, p.1699--1709

    M. Marini, M. Toselli, S. Borsacchi, G. Mollica, M. Geppi, F. Pilati

  48. 2007

  49. Cotton fibers encapsulated with homo- and block copolymers: Synthesis by the atom transfer radical polymerization grafting-from technique and solid-state NMR dynamic investigations
    Biomacromolecules, 2007, 8, p.498-508

    V. Castelvetro, M. Geppi, S. Giaiacopi, G. Mollica

  50. A Novel Polyelectrolyte Complex (PEC) Hydrogel for Controlled Drug Delivery to the Distal Intestine
    The Open Drug Delivery Journal, 2007, 1, p.68-75

    C. Zaino, Y. Zambito, G. Mollica, M. Geppi, M. F. Serafini, V. Carelli, G. Di Colo

  51. Solid-state nuclear magnetic resonance characterization of PE-PEG/Silica hybrid materials prepared by microwave-assisted sol-gel process
    Journal of Materials Research, 2007, 22, p.3516-3525

    M. Geppi, G. Mollica, S. Borsacchi, M. Marini, M. Toselli, F. Pilati

  52. 2006

  53. Molecular properties of flurbiprofen and its solid dispersions with Eudragit RL100 studied by high- and low-resolution solid-state nuclear magnetic resonance
    Pharmaceutical Research, 2006, 23, p.2129-40

    G. Mollica, M. Geppi, R. Pignatello, C. A. Veracini

  54. Truncated dipolar recoupling in solid-state nuclear magnetic resonance
    Chemical Physics Letters, 2006, 432, p.572-578

    I. Marin-Montesinos, G. Mollica, M. Carravetta, A. Gansmüller, G. Pileio, M. Bechmann, A. Sebald, M. H. Levitt

  55. A new hydrogel for the extended and complete prednisolone release in the GI tract
    International Journal of Pharmaceutics, 2006, 310, p.154-161

    G. Di Colo, A. Baggiani, Y. Zambito, G. Mollica, M. Geppi, M. F. Serafini

  56. 2005

  57. Molecular properties of ibuprofen and its solid dispersions with Eudragit RL100 studied by solid-state nuclear magnetic resonance
    Pharmaceutical Research, 2005, 22, p.1544-1555

    M. Geppi, S. Guccione, G. Mollica, R. Pignatello, C.A. Veracini

  58. 2004

  59. Structure and dynamics of flour by solid state NMR: Effects of hydration and wheat aging
    Biomacromolecules, 2004, 5, p.1536-1544

    L. Calucci, L. Galleschi, M. Geppi, G. Mollica